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Advances in Nanostructured Materials...

Rudisill, Stephen G.

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Advances in Nanostructured Materials via Templated Sol-Gel Structure Control and Self-Assembly.

Record Type:	Electronic resources : Monograph/item
Title/Author:	Advances in Nanostructured Materials via Templated Sol-Gel Structure Control and Self-Assembly./
Author:	Rudisill, Stephen G.
Description:	261 p.
Notes:	Source: Dissertation Abstracts International, Volume: 76-10(E), Section: B.
Contained By:	Dissertation Abstracts International76-10B(E).
Subject:	Chemistry. -
Online resource:	http://pqdd.sinica.edu.tw/twdaoapp/servlet/advanced?query=3706943
ISBN:	9781321811940

Advances in Nanostructured Materials via Templated Sol-Gel Structure Control and Self-Assembly.
Rudisill, Stephen G.

Advances in Nanostructured Materials via Templated Sol-Gel Structure Control and Self-Assembly. - 261 p.

Source: Dissertation Abstracts International, Volume: 76-10(E), Section: B.

Thesis (Ph.D.)--University of Minnesota, 2015.

This dissertation describes a body of work focused on understanding and improving morphology control of nanoporous structures via their aqueous chemistry. Synthesis of materials was carried out primarily using the Pechini process with metal nitrates and colloidal crystal templates. CeO2 and CeO 2-derived compounds were used for a substantial portion of the dissertation as they are useful for thermochemical cycling experiments. Templated CeO 2 shows a tenfold improvement over an untemplated material as well as a nanoparticle powder under lab-scale thermochemical cycling experiments.

ISBN: 9781321811940Subjects--Topical Terms:

516420
Chemistry.

Advances in Nanostructured Materials via Templated Sol-Gel Structure Control and Self-Assembly.
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020 $a 9781321811940
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100 1 $a Rudisill, Stephen G. $3 3195123
245 1 0 $a Advances in Nanostructured Materials via Templated Sol-Gel Structure Control and Self-Assembly.
300 $a 261 p.
500 $a Source: Dissertation Abstracts International, Volume: 76-10(E), Section: B.
500 $a Adviser: Andreas Stein.
502 $a Thesis (Ph.D.)--University of Minnesota, 2015.
520 $a This dissertation describes a body of work focused on understanding and improving morphology control of nanoporous structures via their aqueous chemistry. Synthesis of materials was carried out primarily using the Pechini process with metal nitrates and colloidal crystal templates. CeO2 and CeO 2-derived compounds were used for a substantial portion of the dissertation as they are useful for thermochemical cycling experiments. Templated CeO 2 shows a tenfold improvement over an untemplated material as well as a nanoparticle powder under lab-scale thermochemical cycling experiments.
520 $a The Pechini process itself was then investigated as a means to obtain greater structural control over colloidal crystal templated materials. The process was demonstrated to involve phase separation, which allowed for the production of microspheres and bicontinuous networks of templated CeO 2-based solids. Microspheres produced were between 1--3 microm in size, with polydispersity less than 15%. Further experimentation demonstrated that this phase separation methodology was generalizable to Fe2O 3 and Mn3O4, though higher polydispersities were obtained for these materials.
520 $a The final research project accomplished in this dissertation involves a method to produce ordered collagen fibrils through the incorporation of nanocrystalline cellulose during fibrillogenesis. Results were verified via scanning electron microscopy and a mechanism was proposed based on infrared spectroscopy results indicating a decrease in collagen-collagen hydrogen bonding.
590 $a School code: 0130.
650 4 $a Chemistry. $3 516420
650 4 $a Nanoscience. $3 587832
650 4 $a Materials science. $3 543314
690 $a 0485
690 $a 0565
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710 2 $a University of Minnesota. $b Chemistry. $3 1265998
773 0 $t Dissertation Abstracts International $g 76-10B(E).
790 $a 0130
791 $a Ph.D.
792 $a 2015
793 $a English
856 4 0 $u http://pqdd.sinica.edu.tw/twdaoapp/servlet/advanced?query=3706943