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Photodeposition of Gold, Platinum, o...

Taing, James.

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Photodeposition of Gold, Platinum, or Silver onto Titanium Dioxide Nanoparticles at Steps of Highly Oriented Pyrolytic Graphite.

Record Type:	Language materials, printed : Monograph/item
Title/Author:	Photodeposition of Gold, Platinum, or Silver onto Titanium Dioxide Nanoparticles at Steps of Highly Oriented Pyrolytic Graphite./
Author:	Taing, James.
Description:	157 p.
Notes:	Source: Dissertation Abstracts International, Volume: 74-10(E), Section: B.
Contained By:	Dissertation Abstracts International74-10B(E).
Subject:	Chemistry, Physical. -
Online resource:	http://pqdd.sinica.edu.tw/twdaoapp/servlet/advanced?query=3565435
ISBN:	9781303151736

Photodeposition of Gold, Platinum, or Silver onto Titanium Dioxide Nanoparticles at Steps of Highly Oriented Pyrolytic Graphite.
Taing, James.

Photodeposition of Gold, Platinum, or Silver onto Titanium Dioxide Nanoparticles at Steps of Highly Oriented Pyrolytic Graphite. - 157 p.

Source: Dissertation Abstracts International, Volume: 74-10(E), Section: B.

Thesis (Ph.D.)--University of California, Irvine, 2013.

The photodeposition of gold, platinum, or silver nanoparticles selectively onto isolated titanium dioxide (TiO2) nanoparticles created metal/TiO2 photocatalysts and heterogeneous catalysts, and validated the photocatalytic property of the semiconductor. The isolated and ordered TiO2 nanoparticles permitted clear observations of the stability, and changes in morphology, of the particles in various experimental conditions.

ISBN: 9781303151736Subjects--Topical Terms:

560527
Chemistry, Physical.

Photodeposition of Gold, Platinum, or Silver onto Titanium Dioxide Nanoparticles at Steps of Highly Oriented Pyrolytic Graphite.
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100 1 $a Taing, James. $3 2094937
245 1 0 $a Photodeposition of Gold, Platinum, or Silver onto Titanium Dioxide Nanoparticles at Steps of Highly Oriented Pyrolytic Graphite.
300 $a 157 p.
500 $a Source: Dissertation Abstracts International, Volume: 74-10(E), Section: B.
500 $a Adviser: John C. Hemminger.
502 $a Thesis (Ph.D.)--University of California, Irvine, 2013.
520 $a The photodeposition of gold, platinum, or silver nanoparticles selectively onto isolated titanium dioxide (TiO2) nanoparticles created metal/TiO2 photocatalysts and heterogeneous catalysts, and validated the photocatalytic property of the semiconductor. The isolated and ordered TiO2 nanoparticles permitted clear observations of the stability, and changes in morphology, of the particles in various experimental conditions.
520 $a The fabrication of TiO2 nanoparticles at the steps of highly oriented pyrolytic graphite (HOPG), utilizing physical vapor deposition, required heating the graphite substrate to a minimum of 800 °C. The production of a photocurrent, and plating of gold nanoparticles, confirmed the photocatalytic property of the TiO2 nanoparticles on HOPG when utilized as a photoelectrode in a two half-cell setup.
520 $a Employing sodium chloride (1.0 M) as an electrolyte resulted in an increase/decrease of the photocurrent with the addition of gold cations to the half-cell without/with the TiO2 nanoparticles. A poor distribution of gold nanoparticles, roughly 40-45 nm wide, deposited around few of the TiO2 nanoparticles. A lower concentration of sodium chloride (0.1 M) resulted in a coalescence of Au nanoparticles, roughly 10 nm, around many TiO2 nanoparticles.
520 $a Using sodium nitrate as an electrolyte resulted in a rapid decay in the photocurrent and a growth of an unidentified material on the TiO2 nanoparticles. The unidentified material hindered the reduction of gold cations introduced midway through the experiment. With gold cations present at the onset of the experiment, disperse gold nanoparticles (&sim;5-10 nm) deposited around the TiO2 nanoparticles.
520 $a In the absence of additional electrolyte, many disperse gold nanoparticles less than 5 nm deposited onto the TiO2 nanoparticles. More platinum than gold selectively deposited onto the TiO2 nanoparticles. On the contrary, less silver selectively deposited onto the TiO2 nanoparticles.
520 $a Scanning electron microscopy and atomic force microscopy determined the morphology and distribution of the TiO2 nanoparticles and metal/TiO 2 nanocomposites. Energy dispersive X-ray spectroscopy, transmission electron microscopy, and X-ray photoelectron spectroscopy identified the composition of the materials.
590 $a School code: 0030.
650 4 $a Chemistry, Physical. $3 560527
650 4 $a Engineering, Materials Science. $3 1017759
650 4 $a Nanoscience. $3 587832
690 $a 0494
690 $a 0794
690 $a 0565
710 2 $a University of California, Irvine. $b Chemistry - Ph.D.. $3 2094938
773 0 $t Dissertation Abstracts International $g 74-10B(E).
790 $a 0030
791 $a Ph.D.
792 $a 2013
793 $a English
856 4 0 $u http://pqdd.sinica.edu.tw/twdaoapp/servlet/advanced?query=3565435