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Chemical analysis with electrogenera...

Forry, Samuel P.

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Chemical analysis with electrogenerated chemiluminescence.

Record Type:	Electronic resources : Monograph/item
Title/Author:	Chemical analysis with electrogenerated chemiluminescence./
Author:	Forry, Samuel P.
Description:	128 p.
Notes:	Source: Dissertation Abstracts International, Volume: 64-11, Section: B, page: 5492.
Contained By:	Dissertation Abstracts International64-11B.
Subject:	Chemistry, Analytical. -
Online resource:	http://pqdd.sinica.edu.tw/twdaoapp/servlet/advanced?query=3112006

Chemical analysis with electrogenerated chemiluminescence.
Forry, Samuel P.

Chemical analysis with electrogenerated chemiluminescence. - 128 p.

Source: Dissertation Abstracts International, Volume: 64-11, Section: B, page: 5492.

Thesis (Ph.D.)--The University of North Carolina at Chapel Hill, 2003.

Electrogenerated chemiluminescence is the production of excited states through reactions between electrochemically generated intermediates. It can be quite sensitive and useful in chemical analysis. Chapter 1 describes the fundamentals of organic ECL and with examples from the most common organic ECL systems. In Chapter 2, these fundamentals are utilized to allow sensitive and selective ECL detection of some polyaromatic hydrocarbons following liquid chromatographic separation. A derivatization scheme is presented which allows ECL detection of primary amines. Chapter 3 investigates the kinetics of an oxidative-reductive system. This system allows ECL detection in aqueous solutions, but is found to exhibit a slow kinetics. In Chapter 4, detection is demonstrated in a microfluidic device. A method is demonstrated which allows electrochemical measurements in the presence of an electric field without need for a decoupler. Fast scan cyclic voltammetry and ECL detection are demonstrated following electrophoretic separations. In Chapter 5, an approach is presented which facilitates the ECL simulations. Software designed for simulations of electrochemical responses can be used to simulate ECL emission arising from complex mechanisms.Subjects--Topical Terms:

586156
Chemistry, Analytical.

Chemical analysis with electrogenerated chemiluminescence.
LDR:02092nmm 2200253 4500 001 1861413
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035 $a (UnM)AAI3112006
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040 $a UnM $c UnM
100 1 $a Forry, Samuel P. $3 1949014
245 1 0 $a Chemical analysis with electrogenerated chemiluminescence.
300 $a 128 p.
500 $a Source: Dissertation Abstracts International, Volume: 64-11, Section: B, page: 5492.
500 $a Director: R. Mark Wightman.
502 $a Thesis (Ph.D.)--The University of North Carolina at Chapel Hill, 2003.
520 $a Electrogenerated chemiluminescence is the production of excited states through reactions between electrochemically generated intermediates. It can be quite sensitive and useful in chemical analysis. Chapter 1 describes the fundamentals of organic ECL and with examples from the most common organic ECL systems. In Chapter 2, these fundamentals are utilized to allow sensitive and selective ECL detection of some polyaromatic hydrocarbons following liquid chromatographic separation. A derivatization scheme is presented which allows ECL detection of primary amines. Chapter 3 investigates the kinetics of an oxidative-reductive system. This system allows ECL detection in aqueous solutions, but is found to exhibit a slow kinetics. In Chapter 4, detection is demonstrated in a microfluidic device. A method is demonstrated which allows electrochemical measurements in the presence of an electric field without need for a decoupler. Fast scan cyclic voltammetry and ECL detection are demonstrated following electrophoretic separations. In Chapter 5, an approach is presented which facilitates the ECL simulations. Software designed for simulations of electrochemical responses can be used to simulate ECL emission arising from complex mechanisms.
590 $a School code: 0153.
650 4 $a Chemistry, Analytical. $3 586156
690 $a 0486
710 2 0 $a The University of North Carolina at Chapel Hill. $3 1017449
773 0 $t Dissertation Abstracts International $g 64-11B.
790 1 0 $a Wightman, R. Mark, $e advisor
790 $a 0153
791 $a Ph.D.
792 $a 2003
856 4 0 $u http://pqdd.sinica.edu.tw/twdaoapp/servlet/advanced?query=3112006