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Synthesis and applications of hierar...

Sayler, Franchessa Maddox.

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Synthesis and applications of hierarchically porous metal and metal oxide monolithic materials.

Record Type:	Language materials, printed : Monograph/item
Title/Author:	Synthesis and applications of hierarchically porous metal and metal oxide monolithic materials./
作者:	Sayler, Franchessa Maddox.
面頁冊數:	217 p.
附註:	Source: Dissertation Abstracts International, Volume: 74-09(E), Section: B.
Contained By:	Dissertation Abstracts International74-09B(E).
標題:	Engineering, Materials Science. -
電子資源:	http://pqdd.sinica.edu.tw/twdaoapp/servlet/advanced?query=3562456
ISBN:	9781303101120

Synthesis and applications of hierarchically porous metal and metal oxide monolithic materials.
Sayler, Franchessa Maddox.

Synthesis and applications of hierarchically porous metal and metal oxide monolithic materials. - 217 p.

Source: Dissertation Abstracts International, Volume: 74-09(E), Section: B.

Thesis (Ph.D.)--The University of Alabama, 2013.

A nanocasting method for synthesizing a broad range of hierarchically porous, high surface area metal and metal oxide monolithic materials was developed. The importance of a well-connected hard template was established based on conductivity measurements. A hierarchically porous, silica monolith prepared with 7% ocadecyltrimethylammonium bromide was found to be the optimum silica template. Several different factors were found to regulate how well the silica template was replicated. When the connectivity of the silica template, contents of the metal salt solution, impregnation method, temperature, atmosphere, and template removal are all controlled, a good replica of the original silica monolith can be attained in different metals or metal oxides. These metal and metal oxide monoliths were used in catalysis and liquid chromatography.

ISBN: 9781303101120Subjects--Topical Terms:

1017759
Engineering, Materials Science.

Synthesis and applications of hierarchically porous metal and metal oxide monolithic materials.
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100 1 $a Sayler, Franchessa Maddox. $3 2106369
245 1 0 $a Synthesis and applications of hierarchically porous metal and metal oxide monolithic materials.
300 $a 217 p.
500 $a Source: Dissertation Abstracts International, Volume: 74-09(E), Section: B.
500 $a Adviser: Martin G. Bakker.
502 $a Thesis (Ph.D.)--The University of Alabama, 2013.
520 $a A nanocasting method for synthesizing a broad range of hierarchically porous, high surface area metal and metal oxide monolithic materials was developed. The importance of a well-connected hard template was established based on conductivity measurements. A hierarchically porous, silica monolith prepared with 7% ocadecyltrimethylammonium bromide was found to be the optimum silica template. Several different factors were found to regulate how well the silica template was replicated. When the connectivity of the silica template, contents of the metal salt solution, impregnation method, temperature, atmosphere, and template removal are all controlled, a good replica of the original silica monolith can be attained in different metals or metal oxides. These metal and metal oxide monoliths were used in catalysis and liquid chromatography.
590 $a School code: 0004.
650 4 $a Engineering, Materials Science. $3 1017759
650 4 $a Nanotechnology. $3 526235
650 4 $a Nanoscience. $3 587832
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710 2 $a The University of Alabama. $b Chemistry. $3 1679070
773 0 $t Dissertation Abstracts International $g 74-09B(E).
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791 $a Ph.D.
792 $a 2013
793 $a English
856 4 0 $u http://pqdd.sinica.edu.tw/twdaoapp/servlet/advanced?query=3562456